有机氯杀虫剂 EPA 8081A Rtx-CLPesticides2 (双柱分析 Rtx-440)气相色谱图

色谱峰：1六氯环戊二烯Hexachlorocyclopentadiene77-47-42四氯间二甲基苯酚2,4,5,6-TCMX877-09-83顺燕麦敌cis-diallate2303-16-44反燕麦敌trans-diallate2303-16-45α-六六六α-BHC319-84-66六氯苯Hexachlorobenzene118-74-17林丹γ-BHC58-89-98β-六六六β-BHC319-85-79δ-六六六δ-BHC319-86-810七氯Heptachlor76-44-811二氯丙酸Aldrin309-00-212异艾氏剂Isodrin465-73-613环氧七氯Heptachlor epoxide1024-57-3142,4'-DDE2,4'-DDE3424-82-615γ-氯丹γ-Chlordane57-74-916α-氯丹α-Chlordane5103-71-917α-硫丹Endosulfan I959-98-8184,4'-DDE4,4'-DDE72-55-9192,4'-DDD2,4'-DDD53-19-020狄氏剂Dieldrin60-57-121丁酰肼Chlorobenzilate510-15-622安特灵(异狄氏剂)Endrin72-20-8232,4'-DDT2,4'-DDT789-02-6244,4-滴滴滴4,4'-DDD72-54-825β-硫丹Endosulfan II33213-65-926开蓬Kepone143-50-027异狄氏醛Endrin aldehyde7421-93-4284,4'-DDT4,4'-DDT50-29-329硫丹硫酸酯Endosulfan sulfate1031-07-830甲氧滴滴涕Methoxychlor72-43-531异狄氏剂酮Endrin ketone53494-70-532灭蚁灵Mirex2385-85-533间苯二甲腈DCB626-17-5

色谱条件：ColumnsRtx®-CLPesticides230m,0.32mmID,0.50μm(cat.#11325)，SampleOrganochlorinePesticideMixAB#2(cat.#32292)

检测器：ECD（电子捕获检测器）

色谱柱Rtx®-CLPesticides2

色谱柱规格 30m * 0.32mm * 0.50μm ( 长度*内径*膜厚或粒度 )

色谱柱厂家Restek公司

仪器厂家 / 仪器名称：Shimadzu 2010 GC

参考资料：ColumnsRtx®-CLPesticides2 30 m, 0.32 mm ID, 0.50 μm (cat.# 11325)SampleOrganochlorine Pesticide Mix AB #2 (cat.# 32292)Chlorobenzilate (cat.# 32211)Diallate (cis & trans) (cat.# custom)Hexachlorobenzene (cat.# 32231)Hexachlorocyclopentadiene (cat.# 32232)Isodrin (cat.# custom)Kepone (cat.# custom)Mirex (cat.# custom)2,4'-DDD (cat.# 32098)2,4'-DDE (cat.# 32099)2,4'-DDT (cat.# 32200)TCMX (cat.# 32027)Decachlorobiphenyl (BZ #209) (cat.# 32029)InjectionInj. Vol.:1.0 μL splitless (hold 0.75 min)Inj. Temp.:275 °COvenOven Temp.:140 °C (hold 1 min) to 240 °C at 30 °C/min (hold 2 min) to 330 °C at 30 °C/min (hold 4 min)Carrier GasH2, constant pressureLinear Velocity:51 cm/sec @ 140 °CDetectorECD @ 330 °CInstrumentShimadzu 2010 GC