溶剂残留分析 Stabilwax (G16)气相色谱图

色谱峰：溶剂残留分析 Stabilwax (G16)11,1-二氯乙烯1,1-Dichloroethene75-35-421,1,1-三氯乙烷1,1,1-Trichloroethane71-55-63四氯化碳Carbon Tetrachloride56-23-54苯Benzene71-43-251,2-二氯乙烷1,2-Dichloroethane107-06-2

色谱条件：ColumnStabilwax®,30m,0.32mmID,0.25μm(cat.#10624)SampleResidualsolvents-class1(cat.#36279)in20mLheadspacevial(cat.#24685)

检测器：FID

色谱柱Stabilwax®

色谱柱规格 30m * 0.32mm * 0.25μm ( 长度*内径*膜厚或粒度 )

色谱柱厂家Restek公司

仪器厂家 / 仪器名称：GC_PH00951

参考资料：ColumnStabilwax®, 30 m, 0.32 mm ID, 0.25 μm (cat.# 10624)SampleResidual solvents - class 1 (cat.# 36279)in 20 mL headspace vial (cat.# 24685)Diluent:WaterInjectionInj. Vol.:1.0 μL headspace-syringe split (split ratio 5:1)Liner:2 mm splitless (cat.# 20712)Inj. Temp.:140 °CHeadspace-SyringeInstrument:Overbrook Scientific HT200HSyringe Temp.:100 °CSample Temp.:80 °CSample Equil. Time:45 minInj. Speed:8Inj. Dwell:5 sec.OvenOven Temp.:50 °C (hold 20 min) to 165 °C at 6 °C/min (hold 20 min)Carrier GasHe, constant flowFlow Rate:2.15 mL/minLinear Velocity:35.2 cm/secDetectorFID @ 250 °C