潜在遗传毒性分析 Rtx-200气相色谱图

色谱峰：11-氯丙烷1-Chloropropane540-54-52溴乙烷Bromoethane74-96-432-氯丙烷2-Chloropropane75-29-64正丙基溴1-Bromopropane106-94-552-溴丙烷2-Bromopropane75-26-36溴丁烷1-Bromobutane109-65-97硫酸二甲酯Dimethyl sulfate (DMS)77-78-18甲磺酸甲酯Methyl methanesulfonate (MMS)66-27-39甲磺酸乙酯Ethyl methanesulfonate (EMS)62-50-010甲磺酸异丙酯Isopropyl methanesulfonate (iPMS)926-06-711硫酸二乙酯Diethyl sulfate (DES)64-67-512二异丙基硫酸酯di-Isopropyl sulfate (DPS)2973-10-613硫酸二丙酯di-n-Propyl sulfate (DNS)598-05-014硫酸二丁酯Dibutyl sulfate (DBS)625-22-915苯磺酸甲酯Methylbenzene sulfonate (MBS)80-18-216苯磺酸乙酯Ethylbenzene sulfonate (EBS)515-46-817对甲苯磺酸甲酯Methyl toluenesulfonate (MTS)80-48-818ETSEthyl toluenesulfonate (ETS)19苯磺酸正丁酯n-Butyl benzenesulfonate (nBBS)80-44-420nPTSn-Propyl toluenesulfonate (nPTS)21iPTSIsopropyl toluenesulfonate (iPTS)22nBTSn-Butyl toluenesulfonate (nBTS)

色谱条件：ColumnRtx®-200,30m,0.25mmID,1.0μm(cat.#15053)；SampleDiluent:90:10acetonitrile:water；Conc.:100μg/mLInjectionInj.Vol.:1μLsplit(splitratio10:1)Liner:4mmGooseneckSplitlessw/Wool(cat.#22405)；Inj.Temp.:220°C；OvenOvenTemp.:40°C(hold8.3min)to70°Cat70°C/minto115°Cat40°C/minto250°Cat30°C/minto300°Cat15°C/min(hold3min)；CarrierGasHe,constantflow；FlowRate:1mL/min；DetectorMS；Mode:ScanTransferLineTemp.:280°C；IonizationMode:EI；ScanRange:20-250amu；

检测器：MS

色谱柱Rtx®-200

色谱柱规格 30m * 0.25mm * 1.00μm ( 长度*内径*膜厚或粒度 )

色谱柱厂家Restek公司

仪器厂家 / 仪器名称：GC_PH01076